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Center for Nuclear Magnetic Resonance Spectroscopy

University of Florida, Chemistry Department

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Bruker 600 MHz (b600)

located in CLB110

There is a 24 chutes sample changer on the magnet, which you will use to load/unload your sample and to queue samples on automation (iconnmr).

The console is an Avance III HD. It has a Smart probe, with excellent signal-to-noise ratio on both proton and low-band nuclei.

The probe is tuned automatically: this is the instrument you want to use for heteronuclear NMR.

On the b600 you can run 2D experiments with pulsed-field-gradients and shaped pulses, as well as selective 1D experiments. Ask here for a training.

The temperature range is from -150 to 150 C. Ask here for a training.

F19 is on the low-band coil, therefore after tuning to F19 you have to tune back to C13 (and not to H1 as on the Varian instruments). It has the best signal-to-noise ratio for F19 of all the instruments in the Center. This configuration allows for F19-H1 correlation experiments, like HOESY, or observing one of these two nuclei while decoupling the other.

news

  • Variable temperature training May 16, 2025
  • Bruker training May 16, 2025
  • Upcoming trainings May 8, 2025
  • 2D training April 29, 2025
  • Upcoming trainings March 20, 2025
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