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Center for Nuclear Magnetic Resonance Spectroscopy

University of Florida, Chemistry Department

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Bruker 600 MHz (b600)

located in CLB110

The console is an Avance III HD. It has a Smart probe, with excellent signal-to-noise ratio on both proton and low-band nuclei.

There is a 24 chutes sample changer on the magnet, which you will use to load/unload your sample and to queue samples on automation (iconnmr). No automated service yet.

The probe is tuned automatically: this is the instrument you want to use for heteronuclear NMR.

On the b600 you can run 2D experiments with pulsed-field-gradients and shaped pulses, as well as selective 1D experiments. Ask here for a training.

The temperature range is from room temperature to 150 C.

F19 is on the low-band coil, therefore after tuning to F19 you have to tune back to C13 (and not to H1 as on the Varian instruments). It has the best signal-to-noise ratio for F19 of all the instruments in the Center. This configuration allows for F19-H1 correlation experiments, like HOESY, or observing one of these two nuclei while decoupling the other.

news

  • b400 and i3c now open for users November 3, 2020
  • Added runs on Sunday September 17, 2020
  • Labor Day runs September 4, 2020
  • New schedule for the service runs August 31, 2020
  • New schedule for the runs July 31, 2020
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